Abstract
Rotational-echo double resonance (REDOR) is a magic-angle spinning technique for measuring heteronuclear dipolar couplings. Rotor-synchronized π pulses recouple the dipolar interaction. The accuracy of a REDOR determination of distance or orientation depends totally on the quality of the dephased (recoupled) and full-echo spectra. We present a scheme for measuring and compensating for the effects of pulse imperfections in REDOR experiments. No assumptions are made about the quality of the π pulses, and no pulses are added or taken away in implementing the compensation for incomplete REDOR dephasing by imperfect π pulses.
Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
