Abstract

AbstractThe combined rotation and multiple pulse spectroscopy (CRAMPS) experiment is discussed from a practical point of view. Emphasis is given to the understanding of fundamental concepts and practical methods for obtaining optimum results. After a discussion of the basic theoretical concepts of coherent‐averaging theory, the effects of rf pulse errors are discussed. A detailed discussion of spectrometer hardware emphasizes features critical to the success of CRAMPS. A step‐by‐step procedure for spectrometer adjustment in preparation for CRAMPS is outlined. Finally, there is an overview of more sophisticated one‐ and two‐dimensional NMR experiments that incorporate CRAMPS.

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