Combined CFA-AFM Analytical approach for precipitation reaction regarding crystal growth building single and multiple monolayers based on surface area calculation with image surface roughness analysis (unseen surface)

Abstract

A reaction of Mebeverine hydrochloride (0.03mM) in pure form with sodium nitroprusside (0.07mM) to form OFF White precipitate. A constant feed was used to collect an enough amount in weight for AFM study. Continuous flow injection analysis was conducted as it is the aim of this study to combine FIA with AFM. To elucidate the study of surface morphology. Various parameters of AFM image surface roughness analysis were discussed in relation to the kind of precipitate formed. Skewness, kurtosis, peak-peak, ten peak height, fractal dimension, wavelength, core roughness depth, and reduced valley depth. All these with the four parameter mainly amplitude, hybrid, functional and spetial. Since no previous study of such was conducted; all usual mode of imaging was dealt with i.e., contact, non-contact and intermittent contact was defined. A non contact mode was used in this study. A detailed study of how the crystal growth buildup first mono layer (hypothetical based on the date obtained also how much each grain carry a concentration with the number that are on the first mono layer. Number of given samples of surface area calculation plus a demonstration of the hypothetically formed multi mono layers specially at high reactant concentration. The main aim of this project was the binding of AFM with FIA which is regarded as an new approach which might be a very useful knowledge for other researcher.