Abstract
In this work, we describe a new 2D 13C– 13C correlation experiment in solids, in which 13C– 13C J-correlation (COSY) and dipolar correlation (DARR) are recorded at the same time. The sequence is similar to COCONOSY in the liquid-state NMR, in which 1H– 1H COSY and NOESY spectra are obtained in a single experiment. The combined COSY and DARR experiment facilitates assignment of 13C signals in solids.
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