Abstract

Abstract Methyl parathion in technical material, 4 lb/gal. emulsifiable concentrate, and 25% wettable powder was chromatographed on a 1.5% SE-30 + 1.5% OV-210 column with p,p′-DDE as internal standard and flame ionization detection. Three matched sample pairs were analyzed by 15 collaborators using peak height measurements. Liquids were diluted to volume with p,p′-DDE internal standard solution; wettable powders were extracted with chloroform-acetone (9+1), solvent was removed, and extracts were dissolved in internal standard solution. The mean of the coefficients of variation for the 6 samples was 1.65%. The method has been adopted as official first action.

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