Abstract
Abstract The effects of ultrasound (US) agitation (at different intensities of ultrasound) on the codeposition of inorganic fullerene-like (IF) WS 2 in a metallic Ni matrix are investigated. The wt.% of IF-WS 2 particles in the nanocomposite coatings increases from 4.5 wt.% (in films grown under mechanical stirring but without US agitation) up to about 7 wt.% (in films prepared under US agitation at the optimum intensity of ultrasound). While composite coatings obtained only under mechanical stirring exhibit a rather irregular surface morphology, with pronounced 3D multinodular protrusions, a more uniform and compact coating is attained under application of US agitation. In turn, the introduction of WS 2 particles significantly modifies the growth of Ni, inducing grain size refinement, increasing the stacking fault probability and causing a drastic change of crystallographic texture. These microstructural features act in a synergistic manner to simultaneously increase the hardness of the composite coatings while causing the expected decrease in the friction coefficient (due to the presence of WS 2 solid lubricant particles), therefore enhancing the wear resistance, particularly when the coatings are deposited under the presence of US.
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