Abstract
The conditions of synthesis of a new binary complex salt [Co(Cpl)6][Hg2I6] (Cpl is e-caprolactam e-C6H11NO) have been developed, and its structure has been characterized. The salt crystallizes in triclinic system, space group \(P\bar 1\) , a = 10.1078(4) A, b = 12.2680(5) A, c = 13.0782(5) A, α = 62.872(2)°, β = 72.394(2)°, γ = 76.834(2)°, V = 1367.98(9) A3, Z = 1, and ρcalc = 2.297 g/cm3. The structure is insular and consists of isolated ions.
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