Abstract

Loess-paleosol sequences (LPSs) are important terrestrial archives of paleoenvironmental and paleoclimatic information. One of the main obstacles for the investigation and interpretation of these archives is the uncertainty of their age-depth relationship. In this study, four different dating techniques were applied to the Late Pleistocene to Holocene LPS Balta Alba Kurgan (Romania) in order to achieve a robust chronology. Luminescence dating includes analysis of different grain-size fractions of both quartz and potassium feldspar and the best results are obtained using fine-grained quartz blue‐stimulated and polymineral post-infrared infrared-stimulated luminescence measurements. Radiocarbon (14C) dating is based on the analysis of bulk organic carbon (OC) and compound-specific radiocarbon analysis (CSRA). Bulk OC and leaf wax-derived n-alkane 14C ages provide reliable age constraints for the past c. 25–27 kyr. CSRA reveals post-depositional incorporation of roots and microbial OC into the LPS limiting the applicability of 14C dating in older parts of the sequence. Magnetic stratigraphy data reveal good correlation of magnetic susceptibility and the relative paleointensity of the Earth’s magnetic field with one another as well as reference records and regional data. In contrast, the application of paleomagnetic secular variation stratigraphy is limited by a lack of regional reference data. The identification of the Campanian Ignimbrite/Y-5 tephra layer in the outcrop provides an independent time marker against which results from the other dating methods have been tested. The most accurate age constraints from each method are used for two Bayesian age-depth modeling approaches. The systematic comparison of the individual results exemplifies the advantages and disadvantages of the respective methods. Taken as a whole, the two age-depth models agree very well, our study also demonstrates that the multi-method approach can improve the accuracy and precision of dating loess sequences.

Highlights

  • Loess-paleosol sequences (LPSs) are widely spread across Central Eastern Europe (Figure 1) and provide archives of paleoclimate information crucial for the reconstruction of the Pleistocene environmental evolution (e.g., Markovicet al., 2015)

  • In addition to semi-continuous dust input, the formation of LPSs is closely linked to changes in climate and environmental conditions, which are controlled by interglacial-glacial cycles (Gallet et al, 1996; Kohfeld and Harrison, 2003; Svensson et al, 2008; Újvári et al, 2010; Obreht et al, 2017; Zeeden et al, 2018b)

  • In LPSs of the last glacial cycle, the imprint of past climatic fluctuations is preserved as a succession of weakly developed paleosols or pedogenetically overprinted loess layers, which often gradually turn into adjacent loess beds

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Summary

Introduction

Loess-paleosol sequences (LPSs) are widely spread across Central Eastern Europe (Figure 1) and provide archives of paleoclimate information crucial for the reconstruction of the Pleistocene environmental evolution (e.g., Markovicet al., 2015). In LPSs of the last glacial cycle, the imprint of past climatic fluctuations is preserved as a succession of weakly developed paleosols or pedogenetically overprinted loess layers, which often gradually turn into adjacent loess beds. These imprints of orbital to millennial climatic variations provide the backbone for chronostratigraphic correlations (at least) on hemispheric scales and interpretation of deposits across environmental boundaries (e.g., Rousseau et al, 2020). In paleoclimatology, this approach was used even before absolute dating techniques became available (e.g., Emiliani, 1955). In this study we combine absolute dating techniques (optically stimulated luminescence, radiocarbon) with correlative dating (tephrochronology, relative magnetic paleointensity, magnetic susceptibility correlation) and integrate the results in a robust absolute age model

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