Abstract
Chiral and achiral three-dimensional cyanido-bridged metal assemblies with 4-halopyridine, [MnII(4-Xpy)4]2[NbIV(CN)8] (X = I, 1; X = Cl, 2), are prepared. 1 and 2 show ferrimagnetism with TC of 22 and 28 K, respectively. Chiral compound 1 exhibits second-harmonic generation.
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