Abstract

Nucleophilic aromatic substitution of a dialkyl diselenide with 1‐bromo‐2,4‐dinitrobenzene and sodium borohydride in EtOH/THF proceeded chemoselectively in the presence of a thiol, an amine, and a carboxylic acid. ε‐N,N,N‐Trimethyllysine derivative was synthesized from selenohomocysteine dimer by the present arylation, oxidation, cross‐metathesis with 4‐iodobutene, reduction, and substitution with trimethylamine.

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