Abstract
In the presence of CoCl 2 · 6H 2O, the reaction of TCNE (tetracyanoethylene) with CH 3OH forms a dicyanomethylacetate molecule, which has been obtained as one solvent molecule in one new compound {[Co(bpy) 2CN 2][(NC) 2C–CO 2CH 3]} · 2H 2O ( 1). It was characterized by IR spectra, UV–Vis spectra, and cyclic voltammogram. Its structure was determined by X-ray crystallography: 1 crystallizes in P2(1)/ n with a = 13.3368(17), b = 12.5299(16), c = 16.074(2) Å, α = 90, β = 94.6320(10), γ = 90°, and Z = 2.
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