Abstract
AbstractSingle crystals of (Bu4N)8H4 [{Co4(μ3‐OH)4} (SiW10O36)2]·5H2O (I) are precipitated by immersing (Bu4N)6H4 [{Co(H2O)}2(μ3‐OH)2{Co (H2O)2}2 (SiW10O36)2]·5H2O (II) in acetone followed by addition of a 1 M MeOH solution of (Bu4N)OH (313 K, 30 min, 64% yield).
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