Abstract
Abstract[Na(15‐crown‐5)2] [Na(15‐crown‐5)]2(AsMo12O40)·MeCN (I) and [Na(15‐crown‐5)2] [Na(15‐crown‐5)] 2(AsW12O40)·2H2O (II) are solvothermally synthesized from mixtures of Na2MoO4 or Na2WO4, Na3AsO4, MeCN, MeOH, 15‐crown‐5, and HCl solution (autoclave, pH 2.5—3, 120 °C, 48—72 h).
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