Abstract

AbstractYellow‐green block‐shaped crystals of RbUO2(AsO3OH)(AsO2(OH)2) (I) and green block‐shaped crystals of β‐Rb[UO2(AsO3OH)(AsO2 (OH)2)]·H2O (II) are simultaneously hydrothermally synthesized from an aqueous mixture of UO2(NO3)2, RbNO3, and As2O3 in the molar ratio of 1:9:10 (autoclave, 150 °C, 48 h).

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