Abstract
Phosphorylated derivatives of 2-O-α-d-mannopyranosyl-α-d-mannopyranose bearing phosphoric monoesters at OH-6′ (1), OH-6 (2), and at both OH-6 and -6′ (3) were prepared from 8-methoxycarbonyloctyl 2-O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-d-mannopyranosyl)-3,4-di-O-benzyl-6-O- (4-methylphenyldiphenylmethyl)-α-d-mannopyranoside, from which each of the two primary hydroxyl groups was selectively deprotected for subsequent phosphorylation with diphenyl phosphorochloridate.
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