Abstract
AbstractThree chemically distinct clusters built from 32 uranyl peroxide polyhedra, (NH4)40 [(UO2)32(O2)40(OH)24] (I), (NH4)40 [(UO2)32(O2)44(OH)26] (II), and a third one with a composition consistent with coprecipitation of (I) and (II), self‐assemble and crystallize within 15 min from aqueous solutions of uranyl nitrate, ammonium hydroxide, and hydrogen peroxide in different molar ratios under ambient conditions.
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