Abstract
AbstractTwo new hexagonal phases based on brucite‐like octahedral layers with trigonal‐prismatic coordination of interlayer sodium ions, Na0.7Cr0.85Sb0.15O2 (I) and Na0.58Cr0.79Sb0.21O2 (II), are synthesized under flowing argon from mixtures of Na2CO3, Cr2O3, and CrSbO4 (1000—1030 °C, 1—3 h) and characterized by powder XRD and X‐ray fluorescence spectroscopy.
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