Abstract

AbstractThe mixed‐valence uranium(V,VI) oxyhydroxide Na5[U5O16(OH)2] is prepared via reduction of UO22+ under hydrothermal conditions using UO3, NaOH, Na2MoO4 (mineralizer), and Zn as reductant (autoclave, gold ampoule, 570 °C and 150 MPa, 2 d, 50% yield).

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