Abstract
Mass s ectra of the thiocarbonyl-bridged dimers [QMn(CS)(N0)I2 (Q = t7'-C5Hs and $-MeCSH4), [(qS-C,Hs)Fe(CS)(CO)]2, ions, especially those with intact ligands, have been determined. The primary fragmentations in the mass spectra of these complexes have been assigned and compared. Fragment ions resulting from the loss of CO or NO are much more abundant than those resulting from the loss of CS. In fact, a large fraction of the total ion current in the mass spectra of those complexes arises from M2(CS),-containing ions. and (7 P -C,H,),Fe,(CS)(CO), have been examined, and appearance potentials of most of the metal-containing fragment
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