Abstract

AbstractThe fabrication of nanocrystalline A3MF7 (A: K, Na; M: Zr, Hf) is exemplified with Na3ZrF7 starting with a solution of sodium oleate, oleylamine, oleic acid, and ethanolic ZrOCl2 to which an aqueous solution of NH4F and NaF is slowly added (25 °C, 12 h; 83% yield).

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