Abstract
AbstractThe first catalytic asymmetric cycloaddition of carbonyl ylides, derived from diazoketoesters (I), with arylallenes (II) proceeds in a fully chemo‐ and regioselective manner to give 8‐oxabicyclo[3.2.1]octanes (III) (18 examples) with excellent enantio‐ and exo‐diastereoselectivity.
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