Abstract
Abstract(Na,K)16 [(A‐α‐SiW9O34)2Co8 (OH)6(H2O)2(CO3)3] (I) is prepared by addition of a 2 M K2CO3 solution to an aqueous solution of Na10 [A‐α‐SiW9O34]·19H2O and CoSO4 in Na(OAc) (pH 8.9—9.3, 25 °C, 1 h).
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