Abstract

We describe the application of scattering-type near-field optical microscopy to characterize various semiconducting materials using the electron storage ring Metrology Light Source (MLS) as a broadband synchrotron radiation source. For verifying high-resolution imaging and nano-FTIR spectroscopy we performed scans across nanoscale Si-based surface structures. The obtained results demonstrate that a spatial resolution below 40 nm can be achieved, despite the use of a radiation source with an extremely broad emission spectrum. This approach allows not only for the collection of optical information but also enables the acquisition of near-field spectral data in the mid-infrared range. The high sensitivity for spectroscopic material discrimination using synchrotron radiation is presented by recording near-field spectra from thin films composed of different materials used in semiconductor technology, such as SiO2, SiC, SixNy, and TiO2.

Highlights

  • Photons with an energy in the range between terahertz (THz) to ultraviolet can induce a large number of light-matter interactions which can be exploited to gain information about various sample properties

  • We describe the application of scattering-type near-field optical microscopy to characterize various semiconducting materials using the electron storage ring Metrology Light Source (MLS) as a broadband synchrotron radiation source

  • The high sensitivity for spectroscopic material discrimination using synchrotron radiation is presented by recording near-field spectra from thin films composed of different materials used in semiconductor technology, such as SiO2, SiC, SixNy, and TiO2

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Summary

Introduction

Photons with an energy in the range between terahertz (THz) to ultraviolet can induce a large number of light-matter interactions which can be exploited to gain information about various sample properties. The achievable spatial resolution of these optical techniques is, limited by diffraction [1] to about half of the wavelength This prevents to reach a lateral resolution below a few hundred nm when utilizing photons in the visible range, several microns in the mid-infrared (IR) range, and a few hundred microns in the THz range. This limitation can be circumvented by applying nearfield based techniques [2,3,4], such as scattering-type near-field optical microscopy (s-SNOM) [5,6,7,8]. The high sensitivity of this technique and its material discrimination capability are demonstrated by the acquisition of nano-FTIR spectra from materials relevant in semiconductor technology such as SiC, SiO2, TiO2 and SixNy

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