Abstract
Abstract13C CP MAS NMR spectroscopy was used to characterize α‐C:H materials generated from methane and hydrogen mixtures using a microwave plasma. Dipolar dephasing experiments indicate a range of Tdd making quantification of quaternary “diamond”‐like carbons difficult. Unconstrained lineshape analysis is not suitable for the deconvolution of the NMR spectra, but linewidth constrained analyses gave reasonable results. © 1993 John Wiley & Sons, Inc.
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