Characterisation of Fracture and HAC Resistance of an Individual Microstructural Constituent with Micro-Cantilever Testing

Abstract

This paper focuses on the application of miniaturized fracture tests to evaluate the fracture and hydrogen assisted cracking (HAC) resistance of a selected microstructural constituent (acicular ferrite, AF) which only occurs in microscopic material volumes. Site-specific Focused Ion Beam (FIB) micro-machining was used to fabricate sharply notched micro-cantilevers into a region fully constituting of AF. The micro-cantilevers were subsequently tested under uncharged and hydrogen charged conditions with a nanoindenter. The load displacement curves were recorded and analysed with a simplified plastic hinge model for the uncharged specimen, as AF demonstrated an essentially ductile behaviour. The simplified model assisted with FE simulations provided values of the critical plastic crack tip opening displacement (CTOD). A value of the conditional fracture toughness was thereby determined as 12.1 MPa m1/2. With LEFM, a threshold stress intensity factor, Kth, to initiate hydrogen crack propagation in AF was found to range between 1.56 MPa m1/2 and 4.36 MPa m1/2. All these values were significantly below the corresponding values reported for various ferrous alloys in standard macro-tests. This finding indicates that the fracture and HAC resistance at the micro-scale could be very different than at the macro-scale as not all fracture toughening mechanisms may be activated at this scale level.