Abstract

An algorithm of certification of plutonium dioxide by the coulometric method is described. The results of measuring the mass fraction of Pu in PuO2, obtained in certifying and confirming measurements in the course of the development of the state standard sample, are given. The mean mass fraction of Pu in the standard sample material and the uncertainty of the certified value are determined. Based on the results obtained and metrological expertise of the documentation in accordance with GOST (State Standard) 8.315–97, the type of plutonium dioxide composition, SS Pl-tot, is approved, included into the state register, and accepted for use in the Russian Federation.

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