Abstract
In the presence of a catalytic amount of Ni°, 2-methyl-1,3-dioxep-4-ene ( 1) reacts with secondary halogen magnesioamides ( 2) to give mixtures of 4-aminobut-2-enols ( 3) and 2-aminobut-3-enols ( 4), arising from α- or γ-substitution to 1. The stereo- and regiochemistry of the reaction is closely related to the structures of 2.
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