Abstract
The structure of tris(cyclopentadienylcarbonylrhodium) in the solid state has been determined by X-ray diffraction methods. The crystals are monoclinic with a = 7.06, b = 12.92, c = 9.47 Å and β = 94°45′. The structure consists of a triangular arrangement of rhodium atoms with π-cyclopentadienyl groups displaced to one side of the triangle and bridging carbonyl groups on the other. The RhRh distance is 2.62 Å, RhC(ring) 2.24 Å and RhC(carbonyl) 2.00 Å.
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