Abstract
The structure of bis(tetraphenylphosphonium) octa-μ 3 -chloro-hexachlorohexamolybdate(2-) is reported. The structure consists of an [Mo 6 Cl 14 ] 2- cluster anion having a crystallographic center of inversion and two (inversion) symmetry-related tetraphenylphosphonium (TPP) cations. The molybdenum chloride cluster anion is a slightly distorted octahedron of Mo atoms surrounded by eight (μ 3 ) face-bridging and six axial Cl atoms, and is coordinated by ten nearest neighbor TPP molecules. The distorted cluster retains only inversion symmetry
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