Abstract
Electrophilic 1,4-bis(methoxypropyl)-2,3-dimethyl-1,4-diazabutadiene Pd(II) and Pt(II) cations 2a,b with a BArF counteranion have been prepared. Complex 2a undergoes intramolecular C−H activation to form tricyclic 5, and complex 2b adds to Et3SiH to form an octahedral diimine Pt(IV) silyl hydride complex, 7.
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