Abstract

Variable temperature X-ray diffraction (XRD) and real time Fourier transform infrared spectroscopy (FT-IR) were used to study the Brill transition of wekk crystallized Nylon 1012 samples. The experimental data demonstrate that Nylon 1012 undergoes Brill transition at about 120°C. IR spectra also show that a sequence of bands at 897 cm -1 , 986 cm -1 , 1165 cm -1 , 1189 -1 , 1224 cm -1 and 1338 cm -1 which are a-bands disappear abruptly during Brill transition.

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