Abstract
Phosphine compounds [2,6-( t BuOCH 2 ) 2 C 6 H 3 ]PPh 2 ( 1 ) and [2,6-(Me 2 NCH 2 ) 2 C 6 H 3 ]PPh 2 ( 2 ) containing Y,C,Y-chelating ligands were treated with BH 3 ‧SMe 2 . Coordination of BH 3 ·SMe 2 by 2 produced complex {[2,6-(Me 2 NCH 2 ) 2 C 6 H 3 ]Ph 2 P}‧(BH 3 ) 3 ( 3 ). Compound 3 was characterized by means of elemental analyses, 1 H, 11 B, 13 C, 31 P NMR spectroscopy, and by single crystal X-ray diffraction analysis.
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