Abstract
AbstractBis‐perfluoroalkylation of aromatic compounds such as dimethoxybenzenes (2, 4, 6), anisole (8), pyridine (10) and quinoline (13) was accomplished by reaction with excess sodium perfluoroalkanesulfinates, RFSO2Na (1), in the presence of Mn(OAc)3·2H2O under mild conditions. The reaction provides a facile method for the synthesis of bis‐perfluoroalkylated aromatic compounds.
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