Abstract

(E)-9-oxo-2-decenoic acid (queen substance) (1) ;(E)-3,7-dimethyl-2,7-octadienyl propionate (2) and (E)-3,7-dimethyl-2-octene-1,8-diol (3) are easily synthesized via sequential alkylation of bis-(arylsulfonyl) methane 4 with 1,4-allylic substrates 7 and a second electrophile such as 4,4- ethylenedioxy)pentyl iodide and ethyl 2-methylallyl carbonate.

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