Abstract

Biomimetic remineralization is an approach that mimics natural biomineralization, and improves adhesive procedures. The aim of this paper was to investigate the influence of Dentin Caries-like Lesions (DCLL)-Producing Model on microtensile bond strength (μTBS) of etch and rinse adhesive systems and investigate the effect of remineralizing agents such as Sodium Fluoride (NaF), MI Paste™ (MP) and Curodont™ Repair (CR) on caries-affected dentin (n = 6). Nine groups were established: (1) Sound dentin; (2) Demineralized dentin/Chemical DCLL: (3) Demineralized dentin/Biological DCLL; (4) Chemical/DCLL + NaF; (5) Chemical/DCLL + MP; (6) Chemical/DCLL + CR; (7) Biological/DCLL + NaF; (8) Biological/DCLL + MP; (9) Biological/DCLL + CR. Then all dentin blocks were subjected to a bonding procedure with Adper™ Single Bond 2 adhesive system/Filtek Z350XT 4 mm high block, following this they were immersed in deionized water/24 h and then sectioned with ≅1 mm2 beams. The μTBS test was conducted at 1 mm/min/500 N loading. Failure sites were evaluated by SEM (scanning electron microscopy (150×). μTBS data were submitted to factorial ANOVA and Tukey’s test (p < 0.05). The highest values were found when demineralized dentin was treated with MP and CR, regardless caries lesion depth (p < 0.05). There was a predominance of adhesive/mixed in the present study. It was concluded that the use of the artificial dentin caries production models produces differences in the μTBS. Additionally MP and CR remineralizing agents could enhance adhesive procedures even at different models of caries lesion.

Highlights

  • During the execution of routine dental restorations, the hybrid structure formed by the dental bonding procedure occurs through the interaction and subsequent polymerization of monomers around the demineralized collagen matrix [1]

  • To ascertain the potential efficacy of the bonding procedure carried out on remineralized dentin we aimed to evaluate different remineralization treatments and the method used in producing the simulated dentin-like caries lesions on the micro tensile bond strength of remineralized dentin

  • Factorial ANOVA revealed a significant interaction between studied factors: dentin caries-like lesion model and remineralization treatment (p < 0.001)

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Summary

Introduction

During the execution of routine dental restorations, the hybrid structure formed by the dental bonding procedure occurs through the interaction and subsequent polymerization of monomers around the demineralized collagen matrix [1]. Caries is among the most common diseases worldwide [3], and the immediate bond strengths to caries-affected dentin are commonly 20–50% lower than to sound dentin [4,5,6]. Materials 2018, 11, 1733 normal conditions of the mineral content of the caries-affected dentin, prevents the action of enzymes in addition to providing an increased bond durability [7]. Caries-affected dentin is comprised of about 14–53% of water compared with sound dentin, which exhibits a much lower value [8]. By replacing water with minerals at the dentin–resin interface, this would increase the mechanical properties and inhibit water-related hydrolysis [9]

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