Abstract
Abstract Tris(diphenylstibino)amine (Ph2Sb)3N (1) is formed in 49.5% yield by ammonolysis of Ph2SbCl in liquid NH3, and as a side product of the synthesis o f Ph4Sb2 by reactions of Ph3Sb with Na and BrCH2CH2Br in liquid NH3. The structure of 1 was determined by single crystal X-ray diffraction. The crystals consist of molecules with an almost planar Sb3N core (sum of the angles at nitrogen: 352.14°).
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