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Abstract
XPS spectra of a spin-coated film poly(vinyl chloride)(PVC) were collected over a period of 243 min at 303 K to determine specimen damage during long exposures to monochromatic Al Kα x-rays. For this PVC film we measured the loss of chlorine as a function of time by rastering a focused 104.6 W, 100 μm diameter x-ray beam over a 1.4 mm × 0.2 mm area on the sample.
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