Abstract
The main aim of the present work is to study the synthesis and stability of soft-magnetic nanostructured materials under high pressure–high temperature conditions. HITPERM alloy powders were prepared by high-energy ball-milling. The as-milled alloys consist of an iron-based nanocrystalline solid solution. The evolution of crystallinity and grain-size during the ball-milling process and investigations under external pressure up to 3GPa for temperatures up to 1200°C were evaluated using synchrotron radiation X-ray diffraction.
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