Abstract

Due to the high surface area, porosity, and rigidity, applications of nanofibers and nanosurfaces have developed in recent years. Nanofibers and nanosurfaces are typically produced by electrospinning method. In the production process, determination of average fiber diameter is crucial for quality assessment. Average fiber diameter is determined by manually measuring the diameters of randomly selected fibers on scanning electron microscopy (SEM) images. However, as the number of the images increases, manual fiber diameter determination becomes a tedious and time consuming task as well as being sensitive to human errors. Therefore, an automated fiber diameter measurement system is desired. In the literature, this task is achieved by using image analysis algorithms. Typically, these methods first isolate each fiber in the image and measure the diameter of each isolated fiber. Fiber isolation is an error-prone process. In this study, automated calculation of nanofiber diameter is achieved without fiber isolation using image processing and analysis algorithms. Performance of the proposed method was tested on real data. The effectiveness of the proposed method is shown by comparing automatically and manually measured nanofiber diameter values.

Highlights

  • Nanotechnology has recently become the most popular area of scientific and technological activities

  • The following items are used in the electrospinning process: (1) a polymer solution, (2) a feeder that has a low feed rate which is used to transfer the polymer solution to the charging unit, (3) a conductive charging unit that is used to charge the polymer solution, (4) a high voltage power supply to charge the polymer passing through the charging unit, and (5) a grounded connector where the charged polymer is transferred due to the potential difference between charging unit and connector

  • The Multifunctional Electrospinning Platform (MEP) shown in Figure 1 is used in the production process [10]

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Summary

Introduction

Nanotechnology has recently become the most popular area of scientific and technological activities. There are few studies in the literature on automated fiber feature analysis In these studies, fibers were first isolated by using image processing methods. The direction [1, 2], diameter [3–6], pore size [7], uniformity [8], and other structural features [9] of the isolated fibers were investigated. Performance of these studies was tested on both synthetic and real data. Diameters of the real data nanofibers were measured manually for comparison Performance of these methods may be adversely affected by the errors in the fiber isolation process. A novel image analysis method is developed to automate fiber diameter calculation without the need of fiber isolation stage.

SEM Image Analysis Method
Results
Conclusion and Discussion
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