Year-end Sale % OFF 
Abstract
Currently, aberration corrected scanning transmission electron microscopy is a powerful technique to observe with the maximum resolution of all kinds of materials. Unfortunately, this advanced technique has failed in its application to porous solids such as zeolites, which are extremely beam sensitive inorganic solids. By controlling the beam current we have successfully managed to image the most beam sensitive zeolite, zeolite A (LTA type, Si/Al=1) and observe the distribution of silver within the cages, observing for the first time silver octahedra composed of six atoms. These results open up the possibility of applying this technique to any zeolitic framework with the potential capability of even observing the oxygen distribution. Some preliminary results using an annular bright field (ABF) in combination with the HAADF detectors on ZSM-5 (MFI type) zeolite are also presented in this manuscript demonstrating the possibility of obtaining real atomic resolution images of the zeolitic framework.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
