Abstract

Atom location by channelling-enhanced microanalysis (ALCHEMI) has been applied to a Ti2AlNb compound of composition Ti–23 at.% Al–21 at.% Nb so as to deliver absolute compositions for the three sublattices. These compare well with our own neutron diffraction measurements and with previously reported neutron diffraction results. The thus-validated ALCHEMI method has been applied to a single-phase Ti2AlNb compound of composition Ti–27.5 at.% Al–23 at.% Nb annealed at three different temperatures.

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