Asymmetric tensile and compressive creep deformation of hot-isostatically-pressed Y 2O 3-doped -Si 3N 4

Abstract

The uniaxial tensile and compressive creep rates of an yttria-containing hot-isostatically-pressed silicon nitride were examined at several temperatures between 1316 and 1399°C and found to have different stress dependencies. Minimum creep rates were always faster in tension than compression for an equal magnitude of stress. An empirical model was formulated which represented the minimum creep rate as a function of temperature for both tensile and compressive stresses. The model also depicted the asymmetric creep deformation using exponential and linear dependence on tensile and compressive stress, respectively. Unlike other models which represent either tensile or compressive creep deformation as a respective function of tensile or compressive stress, the model in the present study predicted creep deformation rate for both tensile and compressive stresses without conditional or a priori knowledge of the sign of stress. A statistical weight function was introduced to improve the correlation of the model’s regressed fit to the experimental data. Post-testing TEM microstructural analysis revealed that differences in the amount of tensile- and compressive-stress-induced cavitation accounted for the creep strain asymmetry between them, and that cavitation initiated in tensile and compressively crept specimens for magnitudes of creep strain in excess of 0·1%.