Abstract
2-Fluoro-2-deoxy-γ-xylonic and -lyxonic lactones, 7a and 7b, were prepared via the diastereoselective fluorination of the α,β-unsaturated chiral imide 5 followed by dihydroxylation. Lactones 7a and 7b were converted to 2-deoxy-2-fluoro-xylo- d-pyranose ( 1) and 2-deoxy-2-fluoro-lyxo- l-pyranose ( 2) by reduction and deprotection.
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