Abstract
The arene ruthenium(II) azido compounds [{(p-cymene)Ru(N⋂O)N3}] have been prepared by the reaction of [{(p-cymene)Ru(μN3)Cl}2] with the corresponding ligands. The ruthenium azido compounds [{(p-cymene)Ru(N⋂O)N3}] undergo 1,3-dipolar additions with substituted alkynes at room temperature to give the (η6-arene) ruthenium triazolato compounds [(p-cymene)Ru(N⋂O){N3C2(CO2R)2}]. The compounds were characterized on the basis of FTIR, NMR (1H and 13C) and the molecular structure of a representative compound has been established with the help of single crystal X-ray diffraction.
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