Abstract
The preparation of a fluorinated C-glycosidic analogue of a 2-deoxy-2-acetamido- d-altrose is described. The synthetic sequence involves the addition of a difluoroenoxysilane to a d-glucal, an epoxidation of the resulting unsaturated CF 2-glycoside and a ring-opening reaction with TMSN 3. An Overman rearrangement of the unsaturated intermediate is also described.
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