Abstract
An efficient method for the straightforward synthesis of α-fluorinatedacetoxy ketones has been described using fluoro-containing hyper-valent iodine(III) reagents and commercially available alkynes in transition metal-free conditions. This facile procedure exhibits wide substrate applicability and broad functional group tolerance under mild reaction conditions, delivering diverse fluoro-containing α-acetoxyketones in modern to excellent yields. In addition, gram-scale experiments have been accomplished, which promotes its potential applicability.
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