Abstract
The determination of plutonium by eontrolled-potential coulometric titration has been studied and used at Oak Ridge National Laboratory over a period of several years. Two methods-the primary (direct) and secondary (indirect) titrations-have been applied to the analysis of a wide variety of materials. They have been used for the determination of total plutonium, of ionic and polymeric plutonium contents, and of the oxidation state distribution of plutonium solutions. This report describes the techniques, procedures and separations that have been developed. The effects of some contaminants that are common to plutonium-containing samples are also presented.
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