Abstract
AbstractThe suspension polymerization of β‐cyclodextrin (β‐CD) with epichlorohydrin (EP) has been studied using a fractionated factorial design with two levels and six variables (β‐CD:EP molar ratio, NaOH concentration, temperature, stirring speed, delay time before paraffin addition, and β‐CD concentration). Different variables, such as the amount of β‐CD in the product, particle size, degree of swelling, and sorption capacity, have been analyzed as the responses for the synthesized polymers. The experimental design approach permitted to select the optimal conditions of synthesis depending on the desired features of the product. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 3393–3402, 2006
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