Application of allylpalladium intermediate to a simple stereoselective synthesis of (±)-1-hydroxy- trans-8-dodecenoic acid, a precursor of naturally occurring macrolide from cephalosporium recifei

Jiro Tsuji,Tomio Yamakawa,Tadakatsu Mandai

doi:10.1016/s0040-4039(01)85333-8

Application of allylpalladium intermediate to a simple stereoselective synthesis of (±)-1-hydroxy- trans-8-dodecenoic acid, a precursor of naturally occurring macrolide from cephalosporium recifei

Jiro Tsuji, Tomio Yamakawa + Show 1 more

https://doi.org/10.1016/s0040-4039(01)85333-8

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Journal: Tetrahedron Letters	Publication Date: Jan 1, 1978
Citations: 28

Affiliation: Tokyo Institute of Technology

#Simple Synthesis #Simple Stereoselective Synthesis + Show 1 more

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Abstract

Butadien (I) und Nitroethan (II) reagieren in Gegenwart von Pd(O) unter Annahme von Zwischenstufen der Art (III) zu einem Dimeren (IV), das mit Glykol und TiCl3 zum Ketal (V) abgebaut und ketalisiert wird.

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