Abstract
This chapter discusses experimental data of antisolvent content, representing metastable zone width (MSZW) of aqueous ammonium dihydrogen phosphate (ADP) solutions from measurements of solution temperature by feeding of three antisolvents (methanol, ethanol, and acetone). It also discusses MSZW of ethanolic benzoic acid solutions from focused-beam reflectance measurements (FBRM) and ATR-FTIR measurements by feeding antisolvent water as a function of feeding rate. The chapter presents examples of measurements of MSZW by: identification of two different solution temperatures in the plots of temperature of aqueous ADP solution against the antisolvent feeding duration at different rates and identification of occurrence of nucleation event by two different techniques in ethanolic benzoic acid solutions induced by addition of water. It describes the effect of stirring rate on MSZW. The chapter deals with the MSZW of systems involving combined cooling/antisolvent crystallization.
Sign-in/Register to access full text options 
Free) 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a call
